Journal of the Serbian Chemical Society 2022 Volume 87, Issue 9, Pages: 1035-1048
https://doi.org/10.2298/JSC211203058B
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Oxide coatings with immobilized Ce-ZSM5 as visible light photocatalysts
Božović Nikola (University of Belgrade, Faculty of Physics, Belgrade, Serbia + Directorate of Measures and Precious Metals, Belgrade, Serbia)
Mojsilović Kristina 
(University of Belgrade, Faculty of Physics, Belgrade, Serbia)
Stojanović Srna (University of Belgrade, Faculty of Physical, Belgrade, Serbia)
Damjanović-Vasilić Ljiljana (University of Belgrade, Faculty of Physical, Belgrade, Serbia)
Serdechnova Maria (Institute of Surface Science, Helmholtz-Zentrum Hereon, Geesthacht, Germany)
Blawert Carsten (Institute of Surface Science, Helmholtz-Zentrum Hereon, Geesthacht, Germany)
Zheludkevich Mikhail L. (Institute of Surface Science, Helmholtz-Zentrum Hereon, Geesthacht, Germany + Institute of Materials Science, Faculty of Engineering, Kiel University, Kiel, Germany)
Stojadinović Stevan (University of Belgrade, Faculty of Physics, Belgrade, Serbia)
Vasilić Rastko (University of Belgrade, Faculty of Physics, Belgrade, Serbia), [email protected]
The preparation and properties of oxide coatings with immobilized ZSM-5 zeolite obtained by plasma electrolytic oxidation on aluminum support were investigated and discussed. Pure and Ce-exchanged ZSM-5 were immobilized on aluminum supports from a silicate-based electrolyte under ultra-low duty cycle pulsed direct current conditions. The obtained composite coatings were characterized with respect to their morphology, phase and chemical composition, as well as photocatalytic activity and anti-corrosion properties. All mentioned properties of the obtained coatings were dependent on the processing time. The coatings with Ce-exchanged ZSM-5 showed higher photocatalytic activity and more effective corrosion protection than those with pure ZSM-5. The highest photocatalytic activity was observed for coatings processed for 30 min. It is suggested that the surface morphology, Ce-content and number of defects influenced the photocatalytic activity of the composite coatings.
Keywords: plasma electrolytic oxidation, zeolites, multifunctional coatings
Projects of the Serbian Ministry of Education, Science and Technological Development, Grant no. 451-03-68/2022-14/200162 and Grant no. 451-03-68/2022-14/200146
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