Short Note
Version 1
Preserved in Portico This version is not peer-reviewed
(R)-(+)-3,5-dinitro-N-(1-phenylethyl)benzothioamide
Version 1
: Received: 24 April 2023 / Approved: 25 April 2023 / Online: 25 April 2023 (04:18:23 CEST)
A peer-reviewed article of this Preprint also exists.
Donahue, M.G.; Crull, E. (R)-(+)-3,5-Dinitro-N-(1-phenylethyl)benzothioamide. Molbank 2023, 2023, M1650. Donahue, M.G.; Crull, E. (R)-(+)-3,5-Dinitro-N-(1-phenylethyl)benzothioamide. Molbank 2023, 2023, M1650.
Abstract
(R)-(+)-3,5-Dinitro-N-(1-phenylethyl)benzothioamide 1 is a potential chiral solvating agent (CSA) for the spectral resolution of enantiomers by 1H NMR spectroscopy. The single enantiomer of 1 was synthesized from commercially (R)-(+)-a-methylbenzylamine 2 in two-steps with 85% yield.
Keywords
benzylamine; chiral solvating agent; thioamide
Subject
Chemistry and Materials Science, Organic Chemistry
Copyright: This is an open access article distributed under the Creative Commons Attribution License which permits unrestricted use, distribution, and reproduction in any medium, provided the original work is properly cited.
Comments (0)
We encourage comments and feedback from a broad range of readers. See criteria for comments and our Diversity statement.
Leave a public commentSend a private comment to the author(s)
* All users must log in before leaving a comment