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Keywords = frequency sweep keying

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25 pages, 19174 KiB  
Article
Modeling and Evaluation of a Multi-Stable Hybrid Energy Harvester
by Haining Li, Kefu Liu and Jian Deng
Vibration 2024, 7(3), 662-686; https://doi.org/10.3390/vibration7030035 - 1 Jul 2024
Viewed by 305
Abstract
This article develops a multi-stable hybrid energy harvester (MSHEH) which consists of a piezoelectric energy harvester (PEH) and an electromagnetic energy harvester (EMEH). By tuning two parameters, the MSHEH can achieve a mono-stable, bi-stable, and tri-stable state, respectively. A numerical procedure is developed [...] Read more.
This article develops a multi-stable hybrid energy harvester (MSHEH) which consists of a piezoelectric energy harvester (PEH) and an electromagnetic energy harvester (EMEH). By tuning two parameters, the MSHEH can achieve a mono-stable, bi-stable, and tri-stable state, respectively. A numerical procedure is developed to compute the EMEH’s transduction factor. The obtained result is validated experimentally. Using the equivalent magnetic 2-point dipole theory, the restoring force model of the magnetic spring is established. The obtained model is verified experimentally. The energy harvesting performances of the MSHEH under the four different configurations (linear, mono-stable, bi-stable and tri-stable) subjected to frequency sweep excitations are evaluated by simulation and validated by experiment. The comparative analysis focuses on power output, accumulated harvested energy, and effective energy-harvesting bandwidth. The optimum load resistances are investigated by Pareto front optimizations. The following key findings are obtained. When subjected to high-level frequency sweep excitation, the tri-stable configuration exhibits the widest frequency bandwidth and the highest total accumulated harvested energy. When subjected to low-level frequency sweep excitation, the bi-stable configuration is more efficient in energy harvesting. The best performance trade-off between the PEH and EMEH can be achieved by selecting the optimum load resistances properly. Full article
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13 pages, 4516 KiB  
Article
Broadband High-Linear FMCW Light Source Based on Spectral Stitching
by Liang Sun, Xinguang Zhou, Haohao Zhao, Shichang Xu, Zihan Wu, Guohui Yuan and Zhuoran Wang
Photonics 2024, 11(5), 477; https://doi.org/10.3390/photonics11050477 - 19 May 2024
Viewed by 613
Abstract
The key to realizing a high-performance frequency-modulated continuous wave (FMCW) laser frequency-sweeping light source is how to extend the frequency-swept bandwidth and eliminate the effect of nonlinearity. To solve these issues, this paper designs a broadband high-linear FMCW frequency-sweeping light source system based [...] Read more.
The key to realizing a high-performance frequency-modulated continuous wave (FMCW) laser frequency-sweeping light source is how to extend the frequency-swept bandwidth and eliminate the effect of nonlinearity. To solve these issues, this paper designs a broadband high-linear FMCW frequency-sweeping light source system based on the combination of fixed temperature control and digital optoelectronic phase-locked loop (PLL), which controls the temperatures of the two lasers separately and attempts to achieve the coarse spectral stitching based on a time-division multiplexing scheme. Furthermore, we uses the PLL to correct the frequency error more specifically after the coarse stitching, which achieves the spectrum fine stitching and, meanwhile, realizes the nonlinearity correction. The experimental results show that our scheme can successfully achieve bandwidth expansion and nonlinearity correction, and the sweeping bandwidth is twice as much as that of the original single laser. The full-width half-maximum (FWHM) of the FMCW output is reduced from 150 kHz to 6.1 kHz, which exhibits excellent nonlinear correction performance. The relative error of the FMCW ranging system based on this frequency-swept light source is also reduced from 1.628% to 0.673%. Therefore, our frequency-swept light source with excellent performance has a promising application in the FMCW laser ranging system. Full article
(This article belongs to the Special Issue Advanced Lasers and Their Applications II)
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13 pages, 6510 KiB  
Article
Simultaneous Identification of Multiple Parameters in Wireless Power Transfer Systems Using Primary Variable Capacitors
by Chang Liu, Wei Han, Youhao Hu and Bowang Zhang
Appl. Sci. 2024, 14(2), 793; https://doi.org/10.3390/app14020793 - 17 Jan 2024
Viewed by 806
Abstract
This paper proposes a novel approach to simultaneously identifying multiple critical parameters in a wireless power transfer (WPT) system, such as the resonant frequency, mutual inductance, and load resistance, solely from the primary side. The key is to adopt a primary-side-switch-controlled capacitor (SCC) [...] Read more.
This paper proposes a novel approach to simultaneously identifying multiple critical parameters in a wireless power transfer (WPT) system, such as the resonant frequency, mutual inductance, and load resistance, solely from the primary side. The key is to adopt a primary-side-switch-controlled capacitor (SCC) to ensure that the imaginary part of the input impedance is only caused by the secondary-side reflected impedance at three predesigned frequencies. The DSP controller then samples and processes the primary voltage and current using a gradient descent algorithm to derive the above parameters. After the identification, the SCC adjusts its equivalent capacitance based on the secondary-side practical resonant frequency to ensure a zero-phase angle (ZPA), thereby significantly improving the compatibility of the WPT system with unknown receivers. Compared to the previous frequency-sweeping method, the proposed approach is simpler and more suitable for deployment on the controller. Finally, experimental results demonstrate that the identification error of mutual inductance and resonant frequency are within 7.5% and 2.68%, respectively. Full article
(This article belongs to the Special Issue Design and Optimization of Wireless Power Transfer System)
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15 pages, 3044 KiB  
Article
Improved Frequency Sweep Keying CDMA Using Faster R-CNN for Extended Ultrasonic Crosstalk Reduction
by Ga-Rin Park, Sang-Ho Park and Kwang-Ryul Baek
Sensors 2023, 23(23), 9550; https://doi.org/10.3390/s23239550 - 1 Dec 2023
Cited by 1 | Viewed by 733
Abstract
Ultrasonic sensors are inexpensive and provide highly accurate measurements, even with simple hardware configurations, facilitating their use in various fields. When multiple ultrasonic sensors exist in the measurement space, crosstalk occurs due to other nodes, which leads to incorrect measurements. Crosstalk includes not [...] Read more.
Ultrasonic sensors are inexpensive and provide highly accurate measurements, even with simple hardware configurations, facilitating their use in various fields. When multiple ultrasonic sensors exist in the measurement space, crosstalk occurs due to other nodes, which leads to incorrect measurements. Crosstalk includes not only receiving homogeneous signals from other nodes, but also overlapping by other signals and interference by heterogeneous signals. This paper proposes using frequency sweep keying modulation to provide robustness against overlap and a faster region-based convolutional neural network (R-CNN) demodulator to reduce the interference caused by heterogeneous signals. The demodulator works by training Faster R-CNN with the spectrograms of various received signals and classifying the received signals using Faster R-CNN. Experiments implementing an ultrasonic crosstalk environment showed that, compared to on–off keying (OOK), phase-shift keying (PSK), and frequency-shift keying (FSK), the proposed method can implement CDMA even with shorter codes and is robust against overlap. Compared to correlation-based frequency sweep keying, the time-of-flight error was reduced by approximately 75%. While the existing demodulators did not consider heterogeneous signals, the proposed method ignored approximately 99% of the OOK and PSK signals and approximately 79% of the FSK signals. The proposed method performed better than the existing methods and is expected to be used in various applications. Full article
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17 pages, 6018 KiB  
Article
Dynamic Secure Key Distribution Based on Dispersion Equalization and Cellular Automata for Optical Transmission
by Jiabin Cui, Wei Kong, Zhaoyang Liu and Yuefeng Ji
Photonics 2023, 10(12), 1308; https://doi.org/10.3390/photonics10121308 - 27 Nov 2023
Viewed by 1330
Abstract
This paper proposes a dynamic secure key distribution scheme based on dispersion equalization and cellular automata (CAs). The scheme effectively eliminates the key inconsistency problem caused by imperfect channel reciprocity, and dynamic key sequences can be conveniently generated with large key space in [...] Read more.
This paper proposes a dynamic secure key distribution scheme based on dispersion equalization and cellular automata (CAs). The scheme effectively eliminates the key inconsistency problem caused by imperfect channel reciprocity, and dynamic key sequences can be conveniently generated with large key space in long-haul optical transmission. In the process of communication, the legitimate parties obtain the secure core parameter from the frequency domain equalizer algorithm, and a final key sequence is generated through CA iterations on the basis of the core parameter. The randomness and reciprocity characteristics of the channel ensure the security and uniqueness of the core parameter and final key sequence. With 10G Baud 16 quadrature amplitude modulation over 400 km standard single-mode fiber transmission, the proposed scheme is verified with a free key error rate and an unlimited key generation rate. The security robustness of this scheme was theoretically analyzed and verified by sweeping the eavesdropper’s tapping position and improving CA operation processing. The proposed key distribution scheme is compatible with the existing transmission system for different signal modulation formats. Full article
(This article belongs to the Special Issue Optical Communication, Sensing and Network)
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22 pages, 6828 KiB  
Article
Broadband Modelling of Power Transformers for Sweep Frequency Impedance Studies on Winding Short-Circuit Faults
by Yong Liu, Cheng Li, Zhe Guo, Fuqiang Ren, Fei Liu, Yizhe Fu, Yongsheng Zhu and Xiaolei Wang
Electronics 2023, 12(19), 4068; https://doi.org/10.3390/electronics12194068 - 28 Sep 2023
Viewed by 839
Abstract
To study sweep frequency impedance (SFI) features of short-circuit (SC) faults easily, this paper proposes a broadband electric circuit model of a transformer winding and solves its three key problems. The first problem is the calculation of lumped-circuit parameters considering frequency-dependent complex anisotropic [...] Read more.
To study sweep frequency impedance (SFI) features of short-circuit (SC) faults easily, this paper proposes a broadband electric circuit model of a transformer winding and solves its three key problems. The first problem is the calculation of lumped-circuit parameters considering frequency-dependent complex anisotropic permeabilities (FDCAPs), which are caused by the physical characteristics, such as skin, proximity, and geometrical effects and anisotropic properties, of the transformer core and winding materials. The other issue is the establishment of the electric circuit model based on the SFI measurement connection mode, the transformer winding parameters, and a double-ladder network (DLN). Another issue is the construction of the state-space model of the electric circuit toward different SFI values to obtain all network branch voltages and currents. The accuracy of the proposed model is assessed by comparing its SFI signatures with those of the simulation model, without considering FDCAPs under healthy winding, and the corresponding physical transformer model during healthy winding and SC faults. It is observed that the SFI results of the proposed model are closer to the experimental measurements, and the model can be effectively used to study the SFI features of SC faults. Moreover, the impacts of different types of SC faults on the SFI data are concluded in this paper. Full article
(This article belongs to the Section Industrial Electronics)
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11 pages, 2092 KiB  
Article
Parameter Optimization for Modulation-Enhanced External Cavity Resonant Frequency in Fiber Fault Detection
by Xiuzhu Li, Min Zhang, Haoran Guo, Zixiong Shi, Yuanyuan Guo, Tong Zhao and Anbang Wang
Photonics 2023, 10(7), 822; https://doi.org/10.3390/photonics10070822 - 14 Jul 2023
Viewed by 908
Abstract
Fiber fault detection is crucial for maintaining the quality of optical communication, especially in well-established optical access networks with extended distances and a growing number of subscribers. However, the increasing insertion loss in fiber links presents challenges for traditional fault-detection methods in capturing [...] Read more.
Fiber fault detection is crucial for maintaining the quality of optical communication, especially in well-established optical access networks with extended distances and a growing number of subscribers. However, the increasing insertion loss in fiber links presents challenges for traditional fault-detection methods in capturing fault echoes. To overcome these limitations, we propose a modulation-enhanced external-cavity-resonant-frequency method that utilizes a laser for fault echo reception, providing improved sensitivity compared to traditional photodetector-based methods. Our previous work focused on analyzing key parameters, such as sensitivity and spatial resolution, but did not consider practical aspects of selecting optimal modulation parameters. In this study, we develop a model based on Lang–Kobayashi rate equations for current-modulated optical feedback lasers and validate it through experimental investigations. Our findings reveal that optimal detection performance is achieved with a modulation depth of 0.048, a frequency sweeping range of 0.6 times the laser relaxation oscillation frequency, and a frequency sweeping step of 0.1 times the external cavity resonant frequency. Full article
(This article belongs to the Special Issue Fiber Optics and Its Applications)
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16 pages, 10027 KiB  
Article
Nonlinear Dynamics and Energy Harvesting of a Two-Degrees-of-Freedom Electromagnetic Energy Harvester near the Primary and Secondary Resonances
by Krzysztof Kecik and Ewelina Stezycka
Appl. Sci. 2023, 13(13), 7613; https://doi.org/10.3390/app13137613 - 27 Jun 2023
Cited by 5 | Viewed by 1924
Abstract
Energy harvesting is a useful technique for various kinds of self-powered electronic devices and systems as well as Internet of Things technology. This study presents a two-degrees-of-freedom (2DOF) electromagnetic energy harvester that can use environment vibration and provide energy for small electronic devices. [...] Read more.
Energy harvesting is a useful technique for various kinds of self-powered electronic devices and systems as well as Internet of Things technology. This study presents a two-degrees-of-freedom (2DOF) electromagnetic energy harvester that can use environment vibration and provide energy for small electronic devices. The proposed harvester consists of a cylindrical tube with two moving magnets suspended by a magnetic spring mechanism and a stationary coil. In order to verify the theoretical model, a prototype electromagnetic harvester was constructed and tested. The influence of key parameters, including excitation acceleration, response to a harmonic frequency sweep, and electromechanical coupling on the generated characteristics of the harvester, was investigated. The experimental and theoretical results showed that the proposed electromagnetic energy harvester was able to increase the resonance bandwidth (60–1200 rad/s) and output power (0.2 W). However, due to strong nonlinearity, an unstable region occurred near the main first resonance, which resulted from the Neimark–Sacker bifurcation. Full article
(This article belongs to the Special Issue State-of-the-Art in Energy Harvesting for IoT and WSN)
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32 pages, 15537 KiB  
Review
Advances, Challenges, and Future Perspectives of Microwave Reflectometry for Plasma Position and Shape Control on Future Nuclear Fusion Devices
by Bruno Gonçalves, Paulo Varela, António Silva, Filipe Silva, Jorge Santos, Emanuel Ricardo, Alberto Vale, Raúl Luís, Yohanes Nietiadi, Artur Malaquias, Jorge Belo, José Dias, Jorge Ferreira, Thomas Franke, Wolfgang Biel, Stéphane Heuraux, Tiago Ribeiro, Gianluca De Masi, Onofrio Tudisco, Roberto Cavazzana, Giuseppe Marchiori and Ocleto D’Arcangeloadd Show full author list remove Hide full author list
Sensors 2023, 23(8), 3926; https://doi.org/10.3390/s23083926 - 12 Apr 2023
Cited by 6 | Viewed by 2987
Abstract
Providing energy from fusion and finding ways to scale up the fusion process to commercial proportions in an efficient, economical, and environmentally benign way is one of the grand challenges for engineering. Controlling the burning plasma in real-time is one of the critical [...] Read more.
Providing energy from fusion and finding ways to scale up the fusion process to commercial proportions in an efficient, economical, and environmentally benign way is one of the grand challenges for engineering. Controlling the burning plasma in real-time is one of the critical issues that need to be addressed. Plasma Position Reflectometry (PPR) is expected to have an important role in next-generation fusion machines, such as DEMO, as a diagnostic to monitor the position and shape of the plasma continuously, complementing magnetic diagnostics. The reflectometry diagnostic uses radar science methods in the microwave and millimetre wave frequency ranges and is envisaged to measure the radial edge density profile at several poloidal angles providing data for the feedback control of the plasma position and shape. While significant steps have already been given to accomplish that goal, with proof of concept tested first in ASDEX-Upgrade and afterward in COMPASS, important, ground-breaking work is still ongoing. The Divertor Test Tokamak (DTT) facility presents itself as the appropriate future fusion device to implement, develop, and test a PPR system, thus contributing to building a knowledge database in plasma position reflectometry required for its application in DEMO. At DEMO, the PPR diagnostic’s in-vessel antennas and waveguides, as well as the magnetic diagnostics, may be exposed to neutron irradiation fluences 5 to 50 times greater than those experienced by ITER. In the event of failure of either the magnetic or microwave diagnostics, the equilibrium control of the DEMO plasma may be jeopardized. It is, therefore, imperative to ensure that these systems are designed in such a way that they can be replaced if necessary. To perform reflectometry measurements at the 16 envisaged poloidal locations in DEMO, plasma-facing antennas and waveguides are needed to route the microwaves between the plasma through the DEMO upper ports (UPs) to the diagnostic hall. The main integration approach for this diagnostic is to incorporate these groups of antennas and waveguides into a diagnostics slim cassette (DSC), which is a dedicated complete poloidal segment specifically designed to be integrated with the water-cooled lithium lead (WCLL) breeding blanket system. This contribution presents the multiple engineering and physics challenges addressed while designing reflectometry diagnostics using radio science techniques. Namely, short-range dedicated radars for plasma position and shape control in future fusion experiments, the advances enabled by the designs for ITER and DEMO, and the future perspectives. One key development is in electronics, aiming at an advanced compact coherent fast frequency sweeping RF back-end [23–100 GHz in few μs] that is being developed at IPFN-IST using commercial Monolithic Microwave Integrated Circuits (MMIC). The compactness of this back-end design is crucial for the successful integration of many measurement channels in the reduced space available in future fusion machines. Prototype tests of these devices are foreseen to be performed in current nuclear fusion machines. Full article
(This article belongs to the Special Issue Plasma Diagnostics)
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12 pages, 930 KiB  
Article
Characterization of the Anomalous Vibration Response of an Intentionally Mistuned LPT Rotor
by Salvador Rodríguez-Blanco and Carlos Martel
Machines 2023, 11(1), 19; https://doi.org/10.3390/machines11010019 - 24 Dec 2022
Cited by 2 | Viewed by 1327
Abstract
The wind tunnel facility at the Centro de Tecnologías Aeronáuticas was used to perform a set of experiments to study the effect of intentional mistuning on the forced response behavior of an aerodynamically unstable low-pressure turbine rotor. The intentional mistuning patterns were implemented [...] Read more.
The wind tunnel facility at the Centro de Tecnologías Aeronáuticas was used to perform a set of experiments to study the effect of intentional mistuning on the forced response behavior of an aerodynamically unstable low-pressure turbine rotor. The intentional mistuning patterns were implemented by adding a small extra mass to some of the blades. The forced response of the rotor was therefore expected to show two resonance peaks with similar amplitudes, corresponding, respectively, to the vibration frequencies of the blades with and without added mass. However, on the post-processing of the measurements, some anomalous behavior was observed. Near resonance, the system response was synchronous with the forcing, and the frequency sweeps exhibited two resonance peaks, but it was found that the two peaks were clearly different, with the peak at lower frequency showing a much higher vibration amplitude than the high-frequency peak, and with some blades responding at both frequencies with a similar amplitude. In order to give a correct interpretation of the experimental results, a reduced-order model is derived that takes into account only the traveling wave modes coupled by the mistuning. This model, although extremely simple, is capable of reproducing the unexpected behavior of the experiments, and gives a clean explanation of the system response. It is shown that the relative size of the mistuning with respect to the frequency difference of the involved traveling-wave modes is the key parameter for the appearance of this phenomenon. Full article
(This article belongs to the Section Turbomachinery)
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13 pages, 5413 KiB  
Article
A Full Range Experimental Study of Amplitude- and Frequency-Dependent Characteristics of Rubber Springs
by Yanping Shi, Juanjuan Li, Yuan Wang, Xuebing Li, Yuanjing Gao, Dong Zhao, Baohui Shi, Lihua Zou, Xiuduo Song and Yuanyuan Shang
Polymers 2022, 14(21), 4662; https://doi.org/10.3390/polym14214662 - 1 Nov 2022
Cited by 5 | Viewed by 1663
Abstract
This paper provides a comprehensive understanding of the amplitude- and frequency-dependent characteristics of rubber springs. The dynamic nonlinear inelasticity of rubber is a key academic problem for continuum mechanics and a bottleneck problem for the practical use of rubber structures. Despite intensive efforts [...] Read more.
This paper provides a comprehensive understanding of the amplitude- and frequency-dependent characteristics of rubber springs. The dynamic nonlinear inelasticity of rubber is a key academic problem for continuum mechanics and a bottleneck problem for the practical use of rubber structures. Despite intensive efforts witnessed in industrial applications, it still demands an unambiguous constitutive model for dynamic nonlinear inelasticity, which is known as the Payne effect. To this end, three types of rubber springs (shear-type (ST), compression-type (CT) and shear-compression-combination-type (SCCT)) were tested with amplitude and frequency sweeps in different conditions. We investigated and present changes in dynamic stiffness and loss factor with amplitude, frequency and the hysteresis loops of different rubber springs. We also propose a hypothesis and research strategy to study a constitutive model involving multiple factors of hyperelasticity, the Mullins effect, viscoelasticity and the Payne effect, which we hope will provide new ideas for the establishment of a constitutive equation. Full article
(This article belongs to the Section Polymer Applications)
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24 pages, 8940 KiB  
Article
Mechanical Structure Design and Experimental Study of Gamma-ray Monitor for Small Satellite Payload
by Pengfei Guo, Hongbing Xin, Sheng Yang, Shaolin Xiong, Xinqiao Li, Zhenghua An and Dali Zhang
Appl. Sci. 2022, 12(21), 11025; https://doi.org/10.3390/app122111025 - 31 Oct 2022
Viewed by 1582
Abstract
In this paper, a novel mechanical structure for a gamma-ray monitor (GRM) is designed for a small satellite payload. Its structural stiffness, strength and dynamic response are directly related to the performance of the novel GRM, which must meet the static and dynamic [...] Read more.
In this paper, a novel mechanical structure for a gamma-ray monitor (GRM) is designed for a small satellite payload. Its structural stiffness, strength and dynamic response are directly related to the performance of the novel GRM, which must meet the static and dynamic characteristic requirements of the structure in a harsh vibration environment. The static and dynamic simulation of the structure are carried out by finite element method (FEM), and the mechanical structure response laws of the novel GRM are analyzed and validated by vibration tests. Through comparing the frequency response simulation results with the vibration test results, the minimum safety factor of the key components of the structure is 4.07, the fundamental frequency error is within 5.04%, the acceleration response error is within 8.5%, the root mean square of total acceleration (Grms) error is within 14.2%, and the sinusoidal characteristic sweep frequency error before and after the vibration test is within 5.0%. The results show that the payload structure has large structural stiffness, high strength and reasonable frequency response characteristics, and meets the design requirements. Full article
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14 pages, 5125 KiB  
Article
Frequency Sweep Keying CDMA for Reducing Ultrasonic Crosstalk
by Ga-Rin Park, Sang-Ho Park and Kwang-Ryul Baek
Sensors 2022, 22(12), 4462; https://doi.org/10.3390/s22124462 - 13 Jun 2022
Cited by 2 | Viewed by 1747
Abstract
Various sensors are embedded in automobiles to implement intelligent safety technologies such as autonomous driving and front–rear collision avoidance technology. In particular, ultrasonic sensors have been used in the past because they have an accuracy of centimeters to sub-centimeters in air despite their [...] Read more.
Various sensors are embedded in automobiles to implement intelligent safety technologies such as autonomous driving and front–rear collision avoidance technology. In particular, ultrasonic sensors have been used in the past because they have an accuracy of centimeters to sub-centimeters in air despite their low cost and low hardware complexity. Recently, the crosstalk problem between ultrasonic sensors has been raised because the number of ultrasonic sensors in the unit space has increased as the number of vehicles increases. Various studies have been conducted to solve the crosstalk, but a demodulation error occurs when signals overlap. Therefore, in this paper, we propose a method that is robust to ultrasonic signal overlap, is robust even at shorter code length, and has reduced time of flight (TOF) error compared to the existing method by applying frequency sweep keying modulation based on code division multiple access (CDMA). As a result of the experiment, the code was detected accurately regardless of the overlap ratio of the two signals, and it was robust even in situations where the power of the two signals was different. In addition, it shows an accurate TOF estimation even if the ID code length is shorter than the existing on–off-keying, frequency shift keying, and phase shift keying methods. Full article
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17 pages, 4736 KiB  
Article
An Experimental Investigation on the Thermo-Rheological Behaviors of Lactic Acid-Based Natural Deep Eutectic Solvents
by Yousef Elhamarnah, Mashael AlRasheedi, Wadha AlMarri, Asma AlBadr, Alanoud AlMalki, Nora Mohamed, Izzah Fatima, Mustafa Nasser and Hazim Qiblawey
Materials 2022, 15(11), 4027; https://doi.org/10.3390/ma15114027 - 6 Jun 2022
Cited by 4 | Viewed by 2230
Abstract
The rheological studies of Lactic Acid (LA)-based Natural Deep Eutectic Solvents (NADES) are provided in the present investigation. Those mechanisms were also studied in which three distinct Hydrogen Bond Acceptors (HBAs) of Choline Chloride (ChCl), Betaine (Be), and β-Alanine (β-Al), after being added [...] Read more.
The rheological studies of Lactic Acid (LA)-based Natural Deep Eutectic Solvents (NADES) are provided in the present investigation. Those mechanisms were also studied in which three distinct Hydrogen Bond Acceptors (HBAs) of Choline Chloride (ChCl), Betaine (Be), and β-Alanine (β-Al), after being added to a specific Hydrogen Bond Donor (HBD) at a predefined mole-to-mole ratio of 1:1, affected the rheological properties of the prepared NADES. The alterations in the rheology-related characteristics in association with the mechanical and physical properties indicate the tolerance of the material under various operational conditions in the field and show their potential utilization as environmentally suitable and feasible solvents for industrial applications. In the present research, the viscoelastic properties of the three samples of NADES were assessed along with their shear flow properties. The backward and forward temperature change in the Apparent Viscosity (AV) pattern related to the NADES system was described by a rheogram. Furthermore, the density was determined and compared with the AV while considering the temperature-related factor. On a further note, the viscoelastic characteristics were utilized in describing and investigating the network disturbance on the level of the microstructure of NADES upon frequency sweep. A series of experiments were carried out using Thermogravimetry Analysis (TGA) to investigate the thermo-physical properties to optimize them. The rheological properties of shear flow measurements were analyzed using the Bingham model that is best suited for the AV developed with the shear rate with the dynamic yield stress of three systems. The Bingham model was used to determine the lowest stress necessary to disturb the network structure and commence the flow of LA-based NADES. Overall, the viscoelastic behavior of the LA-based NADES revealed the dissimilarity between their strength and viscosity. In addition, shear flow investigations demonstrated that LA-based NADES systems exhibit non-Newtonian properties and substantial shear-thinning effects equivalent to those of alternative IL sorbents. Assessing the rheological properties of LA-based NADES is crucial for a better understanding the key challenges associated with high viscosity. Defining the transport yield stress requirements for NADES systems under different conditions benefits their future development and potentially opens the door to more challenging applications. Full article
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12 pages, 5422 KiB  
Article
Evaluation of the High- and Low-Temperature Performance of Asphalt Mortar Based on the DMA Method
by Yanzhu Wang, Xudong Wang, Zhimin Ma, Lingyan Shan and Chao Zhang
Materials 2022, 15(9), 3341; https://doi.org/10.3390/ma15093341 - 6 May 2022
Cited by 6 | Viewed by 1572
Abstract
Asphalt mortar is a typical temperature-sensitive material that plays a crucial role in the performance of asphalt mixture. This study evaluates the high- and low-temperature performance of asphalt mortar based on the dynamic mechanical analysis (DMA) method. Temperature-sweep tests of asphalt mortars were [...] Read more.
Asphalt mortar is a typical temperature-sensitive material that plays a crucial role in the performance of asphalt mixture. This study evaluates the high- and low-temperature performance of asphalt mortar based on the dynamic mechanical analysis (DMA) method. Temperature-sweep tests of asphalt mortars were conducted using the DMA method under fixed strain level, frequency, and heating rate conditions. The dynamic mechanical response curves, characteristic temperature, and other indices were obtained and used to investigate the high- and low-temperature performance of asphalt mortar. The results showed that the phase transition temperatures T1, T0, and Tg can be used to evaluate the low-temperature performance of asphalt mortar. Additionally, they had a good linear relationship, and the evaluation results were consistent. Meanwhile, T2, E60, and tan(δ)max indicators can effectively evaluate the high-temperature performance of asphalt mortar. Asphalt plays a key role in the performance of asphalt mortar. Mortars with neat asphalt A70 and modified asphalt AR had the worst and best high- and low-temperature performances, respectively. Furthermore, the finer gradation improved the low-temperature performance of asphalt mortar, while the coarser gradation improved the high-temperature properties of modified asphalt mortars but had the opposite effect on neat asphalt A70. Full article
(This article belongs to the Special Issue Performance-Related Material Properties of Asphalt Mixture Components)
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